XD-2 X-Ray Powder Diffractometer - Basic instrument on studying and indentifying the structure

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Updated on: 2015-01-21 17:04
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X-ray Powder  Diffractometer,XD-2

X-ray powder diffractometer is the basic instrument on studying and indentifying the composition and structure of material. The applied field is showed as follows:
 

  • The atom arrangement of all kinds of compound in material could be determined. Some particular performance of material is related with atom arrangement.

  • The composition of material could be determined.

  • The ratio of all kinds compound could be determined.

  • The grain size, stress, texture, orientation and crystallizability.
     


XD-2 is with vertical multifunction goniometer (θ-2θ) which is fit for normal powder and massive solid samples.
The type of vertical θ-2θ goniometer means the X-ray source fixed, the sample stage and detector turned.


Features & Functions

  • Vertical multifunctional high precision goniometer: the minimal step size is 0.00025°. mechanical repeatability excels 0.0006°. θ-2θ goniometer could be selected, which is fit for normal powder and massive solid samples.
  • Easy use and convenient maintenance: the sample is set horizontally because of the vertical goniometer. The sample is more conveniently put in. the sample stage is more conveniently cleaned up. The goniometer will not be polluted and the precision of goniometer is not influenced.
  • High performance: the report of customer operating instrument for 8 months could be provided. The standard deviation of diffraction angle of αSiO2 is better than 0.0015°.
  • Attention to the design of mechanical security: cabinets design and goniometer shutter using a chain institutions, has not yet specified the location of X-ray can not be opened, to prevent leakage of X-ray.
  • A variety of option can extend system functionality: in accordance with the purpose of analysis, you can choose Monochromator Annex and Punch machine.


 

Applications:
 

  • Physics Chemistry
  • Molecular Sieve
  • Battery Materials
  • Environmental Protection- Industrial Waste
  • Ore—Clay—Rocks
  • Petrochemical Industry- Catalyst
  • Iron and Steel
  • Non Ferrous metal
  • Pharmaceuticals
  • Electronic Components
  • Coal – Oil – Natural Gas
  • Ore- Rock
  • Machinery Car Shipbuilding

 

Specifications:

X-ray tube

Type

Cu target, NF model

Focus dimensions

1.0 x10mm²

Maximum power

2KW

X-ray generator

Maximum power

3KW 

X-ray tube voltage

15-60kV

Tube voltage step width

1kV

X-ray tube current

6-50mA

Tube current stop width

1mA

Tube voltage, tube current stability

≤0.01% (Supply voltage fluctuations 10%)

Alarm device

kV low, kV overtop, mA overload, water discharge,

temperature

Ray power protection

0.35, 0.7, 1.0, 1.5, 2.0, 2.7kW six grade

Goniometer

Scanning radius

180mm

Scanning mode

θ-2θ linkage or θ-2θ single move

Measurement range

-182°-180°(θ)

-30°-160°(2θ)

Operation mode

Continuous scanning, Timing Step Scanning, Constant Step Scanning

Continuous scanning speed

0.125°-120°/min

Maximum speed

120°/min

Angle repeatability

0.0006°

Measurement accuracy

0.001°

Minimum step size

0.00025°

Divergence slit (DS)

0.15°, 0.5°, 1°, 2°

Anti- scattering slit (SS)

0.5°, 1°, 2°

Receiving Slit (RS)

0.1,0.15,0.3,0.45,0.6,1,2mm

Zero dedicated slit 

0.02mm

Detection- Counter

The type of detector

Scintillator Counter

 

Crystal type

Nal

 

Pulse- height analyzer(PHA)

Output High Voltage 0-1000V stability ≤0.01% (8h)

Machine cabinet

Cabinet size (mm)

1200(L) x800(W) x1850(H)

Machine weight (kg)

500

Observation window

600(H) x400(W) x10(T)lead glass

X-ray leakage

≤0.1μ Sv/h(non deduction natural

 background)

Safety precautions

Door interlock protection (The door to adesignated location, light gates open only to produce X-ray)

Filter

Ni filter

Corresponding Cu target

Integrated whole stability

 

≤0.3%

Automatic temperature control of circulating water cooling device (indoor unit + outdoor unit)

Model

CW-2F

Cooling power (W)

4000

Power supply

220V, 50Hz

Input power (W)

1800

The largest dimensions (mm)

Indoor Unit

600(L) x400(W) x960(H)

Outdoor Unit

840(L) x300(W) x540(H)

Weight (kg)

Indoor Unit

50

Outdoor Unit

35

Noised B (Indoor Unit)

≤55

Cooling water pressure (MPa)

0-0.7

Cooling water flow (L/min)

≥3.5

Ambient temperature

5℃-40℃

Temperature control range

-49℃-50℃

Temperature control accuracy

±1℃

Warning device

Temperature, water shortage

Optional Accessories & Consumables 

Monochromator Annex

Punch machine


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